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Witt, in Crystal Growth and Characterization, ed. by R. Ueda and J. B. Mullen (North Holland, Amsterdam, 1975) Chapter 10. 5. J. R. Abernathey, D. W. Greenwell, and F. Rosenberger, J. Crystal Growth <47, 145 (1979). 6. F. Rosenberger and G. H. Westphal, J. Crystal Growth 43^, 148 (1978). 7. D. W. Greenwell, B. L. Markham, and F. Rosenberger, J. Crystal Growth 51, 413 (1981). 8. G. H. Westphal and F. Rosenberger, J. Crystal Growth 43, 687 (1978). 9. W. R. Wilcox, J. Crystal Growth 12, 93 (1973).

Nakamura, T. , Bull. Tokyo Inst. , 120, 13 (1974). 18. Horowitz, H. , Longo, J. M. and Lewandowski, J. S. Patent No. 4,129,525 to Exxon Research and Engineering Company (1978). 19. Horowitz, H. , Longo, J. M. and Haberman, J. S. Patent No. 4,124,539 to Exxon Research and Engineering Company (1978). 20. , Atlas of Electrochemical Equilibria in Aqueous Solutions, Pergamon Press, New York, (1966). METASTABLE ALLOYS BY ION IMPLANTATION AND HIGH POWER LASER TREATMENT Animesh K. K. Sood Nuclear Physics Division Bhabha Atomic Research Centre, Bombay, INDIA 1.

A crystallization mechanism of this type would require a finite solubility of the expanded pyrochlores in alkaline media. 26. ~ x x prepared routinely and scale-up to larger batch sizes does not appear to present any problems. 3) are desired, synthesis by the solution route is not as straightforward. 26 will not spontaneously precipitate from the alkaline reaction medium. 26) plus a ruthenium oxide second phase. One possible explanation for this observation is as follows: If a dissolutionreprecipitation mechanism is the route by which a lead ruthenate pyrochlore crystallizes in alkali, it may well be that the solubility of pyrochlores with small degrees of lattice expansion is not high enough for crystallization to occur in a reasonably short time.

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